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• W2953114697 abstract "Single crystals of the new Ba4Mn2NaO9 have been prepared by electrosynthesis in molten NaOH. Its crystal structure has been solved from XRD data (a=10.006(2), c=8.210(3), space group P321, Z=3, R=3.21%, wR=3.52%). It belongs to the wide family of 2H-related perovskite materials and shows columns of face-sharing MnO6 octahedra and NaO6 prisms according to the –(oct–oct–prism)– sequence isolated by Ba2+ cations. The main characteristic of this new oxide is its mixed Mn4+/Mn5+ valence rarely reported up today. Help to the superspace formalism, Ba4Mn2NaO9 (or Ba1+xNaxMn1−xO3 with x=1/3) can be regarded as composed of two interpenetrating sublattices [Ba1+x] and [Na1/3Mn2/3O3] with their own period along the c axis. The ratio γ of these two periods is rational γ=c1/c2=2/3. This composite structure approach which allows us, help to established rules, to predict the crystal structure from the γ-only knowledge has also been pointed out in this work." @default.
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• W2953114697 date "2004-09-01" @default.
• W2953114697 modified "2023-10-17" @default.
• W2953114697 title "Crystal structure of the mixed Mn4+/Mn5+ 2H-perovskite-type Ba4Mn2NaO9 oxide" @default.
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• W2953114697 doi "https://doi.org/10.1016/j.solidstatesciences.2004.05.005" @default.
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