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- W2953214616 abstract "A simple three-step synthetic routes toward 2-substituted 3-diarylmethylenylpiperidines 7 (Y = CN) and 8 (Y = allyl) starting with 3-diarylmethylenylpiperidines 9 is described. The process was carried out by the bromomethoxylation of skeleton 9 with NBS in MeOH at reflux for 2 h, regioselective α-dehydrobromination with DBU in THF at reflux for 10 h, and BF 3 ·OEt 2 -catalyzed cross-coupling of the corresponding enamine with trimethylsilyl-based nucleophiles (TMS-Y) in DCM at rt for 2 h. α - Amino ester 18 and β-amino acid 19 are also synthesized via the simple three-step synthetic protocol." @default.
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- W2953214616 date "2012-02-01" @default.
- W2953214616 modified "2023-09-24" @default.
- W2953214616 title "Regioselective synthesis of 2-substituted 3-diarylmethylenylpiperidines" @default.
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- W2953214616 doi "https://doi.org/10.1016/j.tetlet.2011.11.105" @default.
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