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- W2953230160 abstract "We have found that halogen-exchange occurs effectively between Sn–F and Li–X (X = I, Br, Cl) in tin hydride reagents. This fact induced a complete change in the regiochemistry in the reductions of α,β-unsaturated ketones 1 with Bu2SnH2–Bu2SnF2 (Reagent A): the use of Reagent A in combination with HMPA performed 1,2-reductions, while the addition of LiI to Reagent A achieved 1,4-reductions. It was demonstrated that the regioselectivity of organotin hydrides greatly depends on the properties of the halogen substituents attached to tin atoms." @default.
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- W2953230160 date "1999-03-01" @default.
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- W2953230160 title "A New Halogen-Exchange Reaction between Sn–F and Li–X: Selective 1,2- and 1,4-Reductions of<i>α,β</i>-Unsaturated Ketones and Effects of Halogen Substituents on the Regioselectivity of Organotin Hydrides" @default.
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- W2953230160 doi "https://doi.org/10.1246/bcsj.72.465" @default.
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