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- W2953245737 abstract "Microwave-assisted 1,3-dipolar cycloaddition of (E,E)-1,3-bisarylidenetetral-2-ones with nitrilimines, generated in situ by dehydrohalogenation of the corresponding hydrazonoyl chlorides, affords a series of spiropyrazolines in good to excellent yields. The presence of a second exocyclic CC bond also allows the preparation of dispiropyrazolines. The cycloaddition proceeds with high chemo-, regio- and diastereoselectivity. The structure of the spiranic adducts has been established on the basis of their spectroscopic data and elemental analyses. The stereochemistry of these N-heterocycles has been confirmed by two X-ray diffraction studies. The luminescence properties and fluorescence quantum yields of these heterocyclic compounds have been investigated revealing that some of them are fluorescent in solution." @default.
- W2953245737 created "2019-06-27" @default.
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- W2953245737 date "2016-09-01" @default.
- W2953245737 modified "2023-09-23" @default.
- W2953245737 title "ChemInform Abstract: Stoichiometry-Controlled Cycloaddition of Nitrilimines with Unsymmetrical Exocyclic Dienones: Microwave-Assisted Synthesis of Novel Mono- and Dispiropyrazoline Derivatives." @default.
- W2953245737 cites W2393583318 @default.
- W2953245737 doi "https://doi.org/10.1002/chin.201640134" @default.
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