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- W2953263922 abstract "An efficient synthesis of 1,2-disubstituted acetylenes has been described. Reactions of organoboronic acids with 1,1-dibromo-1-alkenes in the presence of a catalytic amount of CuI (10 mol %), 8-hydroxyquinoline (10 mol %), and using potassium phosphate as base in C2H5OH afforded the desired 1,2-disubstituted acetylenes in good to excellent yields. It is important to note that the formation of 1,3-diynes, which are derived from the homocoupling of 1,1-dibromo-1-alkenes, can be almost completely suppressed under these optimized conditions." @default.
- W2953263922 created "2019-06-27" @default.
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- W2953263922 date "2012-10-01" @default.
- W2953263922 modified "2023-10-06" @default.
- W2953263922 title "Synthesis of 1,2-disubstituted acetylenes via copper-catalyzed Suzuki coupling of organoboronic acids with 1,1-dibromo-1-alkenes" @default.
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- W2953263922 doi "https://doi.org/10.1016/j.tetlet.2012.08.044" @default.
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