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- W2953304427 abstract "A simple, robust and efficient Rh(III)-catalyzed synthesis of novel 12H-indazolo[2,1-a]cinnolin-12-ones has been developed via tandem C–H activation/annulation of 2-phenylindazolones with diazo compounds by using less developed secondary amine as an intrinsic directing group. Notably, a series of nondiscriminating conditions were obtained with excellent test yield. Also, this reaction is highly regioselective with broad substrate scope and both electron-donating and electron-withdrawing groups gave satisfactory yield under very mild conditions (room temperature to 40 °C). It is scalable, compatible with air and H2O, and the only by-products are N2 and H2O. Moreover, the synthesized products represent a new class of fluorophores and their initial spectroscopic characterization has been conducted." @default.
- W2953304427 created "2019-06-27" @default.
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- W2953304427 date "2019-07-01" @default.
- W2953304427 modified "2023-10-14" @default.
- W2953304427 title "Synthesis of Indazolo[2,1-a]Cinnolines via Rhodium (III)-Catalyzed C–H activation/annulation under mild conditions" @default.
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- W2953304427 doi "https://doi.org/10.1016/j.tet.2019.06.021" @default.
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