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- W2953374033 abstract "Abstract A simple and efficient synthetic protocol for the one-pot N-alkylation of nucleobases and their related N-heterocycles via alcohols utilizing the combination of PPh3 and I2 is reported. In this protocol purine, pyrimidine and azole derivatives underwent the N-alkylation reaction with diverse primary alcohols using Ph3P/I2 in the presence of Et3N-K2CO3 in anhydrous DMF to give the N-alkyl adducts (carboacyclic nucleosides) in good yields (up to 90%). The influence of some parameters in this reaction including type of solvent, base, reagents and temperature was discussed. In addition, this protocol has proved the favorable selectivity towards primary hydroxyl versus secondary hydroxyl group in diols." @default.
- W2953374033 created "2019-06-27" @default.
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- W2953374033 date "2016-11-01" @default.
- W2953374033 modified "2023-09-23" @default.
- W2953374033 title "ChemInform Abstract: One-Pot Protocol for N-Alkylation of Purine, Pyrimidine and Azole Derivatives via Alcohols Using Ph3 P/I2 : Simple Route for Carboacyclic Nucleoside Synthesis." @default.
- W2953374033 cites W2460901413 @default.
- W2953374033 doi "https://doi.org/10.1002/chin.201647212" @default.
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