Matches in SemOpenAlex for { <https://semopenalex.org/work/W2955060488> ?p ?o ?g. }
Showing items 1 to 96 of
96
with 100 items per page.
- W2955060488 endingPage "66" @default.
- W2955060488 startingPage "61" @default.
- W2955060488 abstract "A simple procedure based on microextraction by packed sorbent (MEPS) has been proposed for the extraction of dichloropane in oral fluids and its determination by ion mobility spectrometry (IMS). Extraction conditions such as type of sorbent (octyl and octadecyl silica), sample pH, number of sample loadings, and elution volume were evaluated to obtain the most appropriate values. Dichloropane was extracted from saliva samples using C8 MEPS, loading with 100 μL sample (adjusted to pH 7) in 4 cycles, washing with 100 μL deionized water, and eluting with 50 μL 2-propanol in 10 cycles. The proposed MEPS procedure has been validated in terms of linearity, accuracy, and precision. A limit of detection of 30 μg L−1 was obtained for dichloropane determination in saliva. The analysis of field and synthetic saliva samples spiked with dichloropane at concentration levels from 250 to 750 μg L−1 provided relative recoveries between 85 and 110%, using the proposed MEPS-IMS procedure. Field oral fluid samples were collected from healthy individuals, blind-spiked from 92 to 278 μg L−1, and analysed by IMS and gas chromatography-mass spectrometry, being the results obtained from both methods statistically comparable. Thus, the proposed MEPS-IMS procedure involves a simple, sensitive, and accurate analysis of dichloropane in saliva." @default.
- W2955060488 created "2019-07-12" @default.
- W2955060488 creator A5013860366 @default.
- W2955060488 creator A5055830766 @default.
- W2955060488 creator A5072237287 @default.
- W2955060488 creator A5090768439 @default.
- W2955060488 date "2019-10-01" @default.
- W2955060488 modified "2023-09-25" @default.
- W2955060488 title "Determination of the new psychoactive substance dichloropane in saliva by microextraction by packed sorbent – Ion mobility spectrometry" @default.
- W2955060488 cites W1158250007 @default.
- W2955060488 cites W1607280480 @default.
- W2955060488 cites W1969976916 @default.
- W2955060488 cites W2010438378 @default.
- W2955060488 cites W2020096165 @default.
- W2955060488 cites W2022124952 @default.
- W2955060488 cites W2023602932 @default.
- W2955060488 cites W2027190544 @default.
- W2955060488 cites W2063583323 @default.
- W2955060488 cites W2137363620 @default.
- W2955060488 cites W2140458643 @default.
- W2955060488 cites W2142552332 @default.
- W2955060488 cites W2160165060 @default.
- W2955060488 cites W2505586275 @default.
- W2955060488 cites W2662802872 @default.
- W2955060488 cites W2765324982 @default.
- W2955060488 cites W2791023391 @default.
- W2955060488 cites W2802263879 @default.
- W2955060488 cites W2892054910 @default.
- W2955060488 doi "https://doi.org/10.1016/j.chroma.2019.06.054" @default.
- W2955060488 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/31262514" @default.
- W2955060488 hasPublicationYear "2019" @default.
- W2955060488 type Work @default.
- W2955060488 sameAs 2955060488 @default.
- W2955060488 citedByCount "21" @default.
- W2955060488 countsByYear W29550604882019 @default.
- W2955060488 countsByYear W29550604882020 @default.
- W2955060488 countsByYear W29550604882021 @default.
- W2955060488 countsByYear W29550604882022 @default.
- W2955060488 countsByYear W29550604882023 @default.
- W2955060488 crossrefType "journal-article" @default.
- W2955060488 hasAuthorship W2955060488A5013860366 @default.
- W2955060488 hasAuthorship W2955060488A5055830766 @default.
- W2955060488 hasAuthorship W2955060488A5072237287 @default.
- W2955060488 hasAuthorship W2955060488A5090768439 @default.
- W2955060488 hasConcept C119128265 @default.
- W2955060488 hasConcept C150394285 @default.
- W2955060488 hasConcept C15213710 @default.
- W2955060488 hasConcept C162356407 @default.
- W2955060488 hasConcept C178790620 @default.
- W2955060488 hasConcept C185592680 @default.
- W2955060488 hasConcept C205345274 @default.
- W2955060488 hasConcept C2777899863 @default.
- W2955060488 hasConcept C2778533135 @default.
- W2955060488 hasConcept C2778576202 @default.
- W2955060488 hasConcept C43617362 @default.
- W2955060488 hasConcept C4725764 @default.
- W2955060488 hasConcept C504460877 @default.
- W2955060488 hasConcept C55493867 @default.
- W2955060488 hasConcept C73826308 @default.
- W2955060488 hasConceptScore W2955060488C119128265 @default.
- W2955060488 hasConceptScore W2955060488C150394285 @default.
- W2955060488 hasConceptScore W2955060488C15213710 @default.
- W2955060488 hasConceptScore W2955060488C162356407 @default.
- W2955060488 hasConceptScore W2955060488C178790620 @default.
- W2955060488 hasConceptScore W2955060488C185592680 @default.
- W2955060488 hasConceptScore W2955060488C205345274 @default.
- W2955060488 hasConceptScore W2955060488C2777899863 @default.
- W2955060488 hasConceptScore W2955060488C2778533135 @default.
- W2955060488 hasConceptScore W2955060488C2778576202 @default.
- W2955060488 hasConceptScore W2955060488C43617362 @default.
- W2955060488 hasConceptScore W2955060488C4725764 @default.
- W2955060488 hasConceptScore W2955060488C504460877 @default.
- W2955060488 hasConceptScore W2955060488C55493867 @default.
- W2955060488 hasConceptScore W2955060488C73826308 @default.
- W2955060488 hasFunder F4320321864 @default.
- W2955060488 hasLocation W29550604881 @default.
- W2955060488 hasLocation W29550604882 @default.
- W2955060488 hasOpenAccess W2955060488 @default.
- W2955060488 hasPrimaryLocation W29550604881 @default.
- W2955060488 hasRelatedWork W1950305724 @default.
- W2955060488 hasRelatedWork W2036851511 @default.
- W2955060488 hasRelatedWork W2048528605 @default.
- W2955060488 hasRelatedWork W2070691532 @default.
- W2955060488 hasRelatedWork W2078699270 @default.
- W2955060488 hasRelatedWork W2084684145 @default.
- W2955060488 hasRelatedWork W2371004486 @default.
- W2955060488 hasRelatedWork W2566352066 @default.
- W2955060488 hasRelatedWork W2742295280 @default.
- W2955060488 hasRelatedWork W2955060488 @default.
- W2955060488 hasVolume "1603" @default.
- W2955060488 isParatext "false" @default.
- W2955060488 isRetracted "false" @default.
- W2955060488 magId "2955060488" @default.
- W2955060488 workType "article" @default.