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- W2955853072 abstract "NiFe2O4@Co3O4 and ZnFe2O4@Co3O4 core-shell nanoparticles were synthesized and reduced to be used as catalysts for the Fischer-Tropsch synthesis. The as-synthesized materials were determined to have an incomplete Co3O4 shell around the ferrite core with a maximum thickness of 3 nm. Using in-situ TEM, it was shown that reduction of these core-shell nanoparticles in pure hydrogen at 230 °C and 250 °C, respectively, resulted in the formation of small cobalt islands on the ferrite surface. Catalytic testing of the core-shell materials, NiFe2O4@Co3O4 and ZnFe2O4@Co3O4, after reduction showed a cobalt-time yield of 13.64 μmolCO·gCo−1·s−1 and 4.27 μmolCO·gCo−1·s−1 and a C5+ selectivity of 47 C-% and 68 C-%, respectively. The observed difference in cobalt-time yield and selectivity between NiFe2O4@Co3O4 and ZnFe2O4@Co3O4 core-shell nanoparticles was ascribed to a combination of effects that arose from the morphological and compositional changes that occurred after reduction and under Fischer-Tropsch synthesis conditions." @default.
- W2955853072 created "2019-07-12" @default.
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- W2955853072 date "2019-09-01" @default.
- W2955853072 modified "2023-10-17" @default.
- W2955853072 title "Morphological and compositional changes of MFe2O4@Co3O4 (M = Ni, Zn) core-shell nanoparticles after mild reduction" @default.
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- W2955853072 doi "https://doi.org/10.1016/j.matchar.2019.109806" @default.
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