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- W2956083105 abstract "In this study, a vortex-assisted liquid–liquid microextraction procedure for simultaneous determination of three carbamate pesticides (desmedipham, phenmedipham and chlorpropham) was developed and for a first time was combined with high-performance liquid chromatography with amperometric detection (HPLC-AD) on a glassy carbon electrode. Variables that affect the procedure were studied, and optimal conditions were found to be 125 μL of toluene as the extraction solvent, 60 s of vortexing at 3000 rpm and a 3 mL sample volume. The HPLC-AD measurements were carried out using the gradient elution method, with a mobile phase consisting of methanol, a buffer solution at pH 3 and detection potential of +1.3 V. The developed method was successfully applied for the analysis of two types of samples: aqueous (wine, beer, apple juice) and solid (potato)." @default.
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- W2956083105 date "2019-11-01" @default.
- W2956083105 modified "2023-09-26" @default.
- W2956083105 title "Simultaneous determination of three carbamate pesticides using vortex-assisted liquid–liquid microextraction combined with HPLC-amperometric detection" @default.
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- W2956083105 doi "https://doi.org/10.1016/j.microc.2019.104071" @default.
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