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- W2956245114 abstract "The synthesis of 3-formylindole labelled in the formyl group withdeuterium or tritium has been achieved via pyrolysis of the deuteriatedor tritiated anilinium salt of indole-3-glyoxylic acid. The, labelledaldehydes have been used to prepare tryptophan stereoselectivelylabelled with deuterium or tritium in the β-methylene group by theoxazolinone method. The configurations of the labelled tryptophanswere established by 1H n.m.r. spectroscopy of the deuteriated compoundsand by chemical and enzymic degradation of the tritiated compounds tofumaric acid via 4,7-dihydrotryptophan and aspartic and malic acids.In addition, biosynthetic conversion of the tritiated compounds intothe antibiotic indolmycin has confirmed the assignments of configurationand established stereochemical purities of ca. 94%. [Continues.]" @default.
- W2956245114 created "2019-07-23" @default.
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- W2956245114 date "1975-01-01" @default.
- W2956245114 modified "2023-09-27" @default.
- W2956245114 title "The biosynthesis of fungal metabolites derived from tryptophan" @default.
- W2956245114 hasPublicationYear "1975" @default.
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