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• W2959480887 startingPage "1654" @default.
• W2959480887 abstract "Coordination-driven self-assembly (CDSA) is increasingly used to synthesize coordination complexes containing metal-centered electron acceptors and typically nitrogen-containing electron donors. Characterization of the structures obtained from CDSA via crystallographic or spectroscopic means is limited due to difficulties in forming single crystals for X-ray studies and overlapping precursor and product signals in NMR. Here, we employ ion mobility-mass spectrometry (IM-MS), which provides a direct measure of size and shape of the CDSA complexes, to study the intact reaction products of a rhomboid-shaped complex. This approach negates the need for product isolation and crystallization and allows for tracking of the product distribution as a function of time. A potential challenge of IM-MS is that the size/shape of the observed CDSA complexes can vary with internal energy; however, we show that proper tuning of the instrument reduces the effects of collisional activation thereby allowing for retention of ion conformations that reflect solution-phase ion structures." @default.
• W2959480887 created "2019-07-23" @default.
• W2959480887 creator A5009839117 @default.
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• W2959480887 date "2019-07-17" @default.
• W2959480887 modified "2023-09-23" @default.
• W2959480887 title "Topological Characterization of Coordination-Driven Self-assembly Complexes: Applications of Ion Mobility-Mass Spectrometry" @default.
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• W2959480887 doi "https://doi.org/10.1007/s13361-019-02276-6" @default.
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• W2959480887 hasPublicationYear "2019" @default.
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