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- W2959576720 abstract "Abstract A novel energetic polymer binder was developed through ring opening copolymerization of 3-nitratomethyl-3-methyloxetane (NIMMO) with (HTPE) as a macroinitiator to form tri-block copolymer polyNIMMO-HTPE-polyNIMMO. The structure of tri-block copolymer was confirmed by FTIR, 1H NMR, 13C NMR and GPC. In comparison with HTPE, polyNIMMO-HTPE-polyNIMMO has a higher viscosity because of its increased molecular weight with additional ONO2 as side groups and strengthened intermolecular interaction. The glass transition temperature studies show two glass transition processes in their DSC curves. One signal around −69 °C arises from the HTPE segment, while the other signal around −30 °C is related to the terminal polyNIMMO segments in the tri-block polymers. The TGA-DTG and DSC curves indicate that polyNIMMO-HTPE-polyNIMMO has a good thermal stability and its exothermic decomposition peak is found to be around 220 °C. The kinetic parameters and the thermodynamic parameters for the thermal decomposition of polyNIMMO-HTPE-polyNIMMO-IV are obtained from the DSC data by non-isothermal methods proposed by ASTM E698 and FWO. These results demonstrate that tri-block copolymer polyNIMMO-HTPE-polyNIMO might be a potential energetic propellant binder." @default.
- W2959576720 created "2019-07-23" @default.
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- W2959576720 date "2019-10-01" @default.
- W2959576720 modified "2023-09-26" @default.
- W2959576720 title "PolyNIMMO-HTPE-polyNIMMO triblock copolymer as a potential energetic binder: Synthesis and characterization" @default.
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- W2959576720 doi "https://doi.org/10.1016/j.eurpolymj.2019.07.014" @default.
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