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- W2959935224 abstract "1,2-Limonene oxide was synthesized for the first time via epoxidation reactions of (R)-(+)-limonene mediated by a new immobilized preparation with low-cost material from Candida antarctica lipase fraction B (NS 88011). Parameters affecting this reaction were studied, such as enzyme amount, acyl donor concentration, oxidant concentration, (R)-(+)-limonene concentration, reaction time, and temperature. The synthesis was maximized in fed-batch reactors, considering 40 mM (R)-(+)-limonene, 70 mM octanoic acid, and 250 mM H2O2 (35% aqueous solution). NS 88011 and Novozym 435 led to similar results, which makes NS 88011 a promising and low-cost alternative in epoxidation reactions mediated by lipase. The best result in the 1,2-limonene oxide synthesis was 74.92 ± 1.12% of yield at 40 min. In addition, both NS 88011 and Novozym 435 can be used for up to three cycles. Therefore, NS 88011 had a good and viable performance in the epoxidation reactions of the (R)-(+)-limonene and after purification led to a final product with purity >95%." @default.
- W2959935224 created "2019-07-23" @default.
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- W2959935224 date "2019-07-15" @default.
- W2959935224 modified "2023-09-23" @default.
- W2959935224 title "Epoxidation of (<i>R</i>)-(+)-Limonene to 1,2-Limonene Oxide Mediated by Low-Cost Immobilized <i>Candida antarctica</i> Lipase Fraction B" @default.
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- W2959935224 doi "https://doi.org/10.1021/acs.iecr.9b02168" @default.
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