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• W2960370413 abstract "Sulfonyl fluorides are valuable synthetic motifs for a variety of applications, among which sulfur(VI) fluoride exchange-based click chemistry is currently the most prominent. Consequently, the development of novel and efficient synthetic methods to access these functional groups is of great interest. Herein, we report a mild and environmentally benign electrochemical approach to prepare sulfonyl fluorides using thiols or disulfides, as widely available starting materials, in combination with KF, as an inexpensive, abundant and safe fluoride source. No additional oxidants nor additional catalysts are required and, due to mild reaction conditions, the reaction displays a broad substrate scope, including a variety of alkyl, benzyl, aryl and heteroaryl thiols or disulfides." @default.
• W2960370413 created "2019-07-23" @default.
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• W2960370413 date "2019-07-13" @default.
• W2960370413 modified "2023-10-16" @default.
• W2960370413 title "Sulfonyl Fluoride Synthesis through Electrochemical Oxidative Coupling of Thiols and Potassium Fluoride" @default.
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• W2960370413 doi "https://doi.org/10.1021/jacs.9b06126" @default.
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• W2960370413 hasPublicationYear "2019" @default.
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