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- W2963310873 endingPage "102517" @default.
- W2963310873 startingPage "102517" @default.
- W2963310873 abstract "Optimum sintering temperature (Ts) plays an important role in controlling densification and growth of grains which greatly affect the magnetic and electrical properties of polycrystalline materials. Y-substituted Mg-Zn [Mg0.5Zn0.5YxFe2−xO4 (0 ≤ x ≤ 0.05)] ferrites have been prepared by using conventional standard ceramic technique and were sintered between 1100 and 1300 °C in the steps of 50 °C. Characterizations of the samples have been done by X-ray diffraction (XRD) technique, field emission scanning electron microscopy (FESEM), dielectric and permeability measurements to find the suitable Ts. XRD data have been analyzed and the results confirmed the same information regarding phase analysis at different Ts. Further characterization of the samples, sintered at 1100 and 1150 °C, were not continued due to their low density and high porosity. FESEM images indicate the change in microstructure with Ts. The decrease (increase) of ac electrical resistivity with Ts (Y content) has been observed while the dielectric constant behaves in opposite manner. Impedance spectroscopy also exhibited similar trend as ac electrical resistivity. The initial permeability revealed the wide stability zone of frequency and different optimum Ts for different compositions. The ac resistivity values for the compositions have been found higher at 1200 °C, but the compositions have highest value of bulk density and permeability at other Ts. The effect of Ts on the physical properties (bulk density, porosity and permeability) of Y-substituted Mg0.5Zn0.5YxFe2−xO4 (0 ≤ x ≤ 0.05) ferrites elucidate that the optimum Ts should be of 1250 °C for x = 0.01, 0.02 and 0.03 while the Ts should be of 1300 °C for x = 0.04 and 0.05." @default.
- W2963310873 created "2019-07-30" @default.
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- W2963310873 date "2019-09-01" @default.
- W2963310873 modified "2023-10-06" @default.
- W2963310873 title "Study of physical properties towards optimizing sintering temperature of Y-substituted Mg-Zn ferrites" @default.
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- W2963310873 doi "https://doi.org/10.1016/j.rinp.2019.102517" @default.
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