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• W2964863644 startingPage "113363" @default.
• W2964863644 abstract "Use of a rotating ring-disk electrode during gas-evolving reactions has been shown liable to errors under higher current densities, since product collection on the ring is vulnerable to the formation of gas bubbles at the disk-ring interspace. In this study, we explored methods of reducing such bubble-related errors and improving the reliability of the collection factor under high-intensity gas evolution. We attempted the mounting of a thin wire close to the surface, to dislodge bubbles that formed specifically on the interface between the disk and the disk-ring spacer. This approach was tested for the detection of chlorine during parallel chlorine and oxygen evolution, and resulted in a notable alteration of the collection efficiency; its value became lower than theoretical expectations and also quite stable, even under higher current densities. We also coated the RRDE tip in a hydrophilic polymer, to reduce the tendency of bubble formation; this was tested for the collection of hydrogen and oxygen gas, and led to a mild increase in overall performance. The coating allowed for approximately 50% higher hydrogen evolution current density without ring failure, and for oxygen collection led to an overall improvement in behaviour." @default.
• W2964863644 created "2019-08-13" @default.
• W2964863644 creator A5028485156 @default.
• W2964863644 creator A5054611790 @default.
• W2964863644 date "2019-10-01" @default.
• W2964863644 modified "2023-10-12" @default.
• W2964863644 title "Examination and prevention of ring collection failure during gas-evolving reactions on a rotating ring-disk electrode" @default.
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• W2964863644 doi "https://doi.org/10.1016/j.jelechem.2019.113363" @default.
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