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• W2965251567 abstract "The incommensurately modulated crystal structure of the mineral daliranite has been determined using 3D electron diffraction data obtained on nanocrystalline domains. Daliranite is orthorhombic with a = 21, b = 4.3, c = 9.5 Å and shows modulation satellites along c . The solution of the average structure in the Pnma space group together with energy-dispersive X-ray spectroscopy data obtained on the same domains indicate a chemical formula of PbHgAs 2 S 5 , which has one S fewer than previously reported. The crystal structure of daliranite is built from columns of face-sharing PbS 8 bicapped trigonal prisms laterally connected by [2+4] Hg polyhedra and (As 3+ 2 S 5 ) 4− groups. The excellent quality of the electron diffraction data allows a structural model to be built for the modulated structure in superspace, which shows that the modulation is due to an alternated occupancy of a split As site." @default.
• W2965251567 created "2019-08-13" @default.
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• W2965251567 date "2019-07-22" @default.
• W2965251567 modified "2023-09-25" @default.
• W2965251567 title "Daliranite, PbHgAs₂S₅: determination of the incommensurately modulated structure and revision of the chemical formula" @default.
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• W2965251567 doi "https://doi.org/10.1107/s2052520619007340" @default.
• W2965251567 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/32830727" @default.
• W2965251567 hasPublicationYear "2019" @default.
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