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• W2966015125 endingPage "151687" @default.
• W2966015125 startingPage "151687" @default.
• W2966015125 abstract "In this work, in situ ZrC/Si-B-C-N monoliths prepared by sol-gel and reactive hot-pressing techniques were developed. The fine ZrC powders were synthesized by decomposition of zirconium propanol and furfuryl alcohol using as the source of zirconium and carbon, respectively. The as-sintered ZrC/Si-B-C-N monoliths composed of ZrC, SiC and BN(C) with a very fine and homogenous microstructure. The in situ formed ZrC and SiC were equiaxed, whereas the in situ BN(C) was graphic hexagonal with a fake-like structure. Due to the poor sinterability of ZrC, the as-sintered monoliths with relative low densities of <80% were obtained, which was primarily responsible for the poor mechanical performance. ZrC/Si-B-C-N monoliths oxidized at 1500 °C for different time possessed the same oxidation products of ZrO2 and ZrSiO4. SiC and BN(C) oxidation are predicted thermodynamically more strongly than ZrC, which resulted in a thick, uneven, heterogenous and porous oxide scale. The introduction of ZrC weakens the oxidation resistance of Si-B-C-N matrix leading to a continuous weight gain." @default.
• W2966015125 created "2019-08-13" @default.
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• W2966015125 date "2019-11-01" @default.
• W2966015125 modified "2023-10-17" @default.
• W2966015125 title "In situ ZrC/Si-B-C-N monoliths prepared by sol-gel and reactive hot-pressing: Processing, microstructure, mechanical properties and oxidation behavior" @default.
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• W2966015125 doi "https://doi.org/10.1016/j.jallcom.2019.151687" @default.
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