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• W2967134243 abstract "A base-mediated trans-hydroboration of propiolamides that provides access to previously elusive primary and secondary (E)-β-borylacrylamide products has been developed. In the presence of n-butyllithium and pinacolborane, complete regioselectivity and stereoselectivity is observed, affording the corresponding vinylboronate products in up to 91% yield. A wide variety of primary and secondary amides served as efficient substrates for this transformation. A plausible reaction mechanism that involves substrate-assisted activation and a key intramolecular cyclization is discussed." @default.
• W2967134243 created "2019-08-22" @default.
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• W2967134243 date "2019-08-08" @default.
• W2967134243 modified "2023-09-26" @default.
• W2967134243 title "<i>trans</i>-Hydroboration of Propiolamides: Access to Primary and Secondary (<i>E</i>)-β-Borylacrylamides" @default.
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• W2967134243 doi "https://doi.org/10.1021/acs.orglett.9b02408" @default.
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