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• W2967201843 abstract "The synthesis of ZnO nanoparticles proceeds through a complex sequence of precursor reactions, nucleation, and growth processes. For further advancement and control of nanoparticle synthesis, a detailed understanding of the mechanisms and kinetics is essential. With the recent advancement in X-ray scattering and spectroscopy methods, in situ experiments during nanoparticle synthesis can be performed, which provide important new insights into reaction and growth mechanisms. Here we use in situ small- and wide-angle X-ray scattering (SAXS, WAXS) coupled with UV-vis spectroscopy to investigate the nucleation and growth process of an oleate-based ZnO nanoparticle synthesis yielding narrowly disperse nanoparticles over the complete time scale from 30 s to 18 h. We find that the nucleation and early growth period during the first 1000 s can be quantitatively described by a classical homogeneous nucleation and growth mechanism. Furthermore, we identified a second growth phase where nanoparticle crystallization occurs, as indicated by the appearance of higher-order Bragg peaks and a pronounced shift of the absorption edge in the UV-vis spectra. The results are in very good agreement with recent studies on the use of the ZnO alkali hydroxide hydrolysis route. Thus, a very good understanding of the nucleation and growth mechanisms and kinetics of the most important ZnO synthesis routes has been established." @default.
• W2967201843 created "2019-08-22" @default.
• W2967201843 creator A5025759143 @default.
• W2967201843 creator A5034812442 @default.
• W2967201843 creator A5048997398 @default.
• W2967201843 date "2019-08-12" @default.
• W2967201843 modified "2023-09-27" @default.
• W2967201843 title "Nucleation and Growth Kinetics of ZnO Nanoparticles Studied by in Situ Microfluidic SAXS/WAXS/UV–Vis Experiments" @default.
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• W2967201843 doi "https://doi.org/10.1021/acs.langmuir.9b01149" @default.
• W2967201843 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/31403801" @default.
• W2967201843 hasPublicationYear "2019" @default.
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