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• W2967744904 abstract "In this work, a convenient, sensitive method for simultaneous monitoring of malachite green, leucomalachite green in tilapia samples was developed by ultra-high-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). The tilapia samples were extracted by acetonitrile, separated withacetonitrile-5mmol/L ammonium acetate as mobile phase, and then detected under ESI+ mode. The method showed a good linearity for all the analysts over the range of 0.1-100 μg kg-1 with r2≥0.998. And the detection limits both were 0.10 μg kg-1 for Malachite green and leucomalachite green. Tests for recovery were made by addition of standards at four different concentration levels (0.5, 2.0, 10.0, 20.0 μg kg-1) to the blank sample. The recoveries of the four spiked concentrations were ranged from 81.5% to 104%, with the relative standard deviations lower than 5%. The sensitivity, accuracy and precision of this method were able to meet the requirements for malachite green and leucomalachite green residue analysis." @default.
• W2967744904 created "2019-08-22" @default.
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• W2967744904 date "2019-07-01" @default.
• W2967744904 modified "2023-09-23" @default.
• W2967744904 title "Application of UPLC-MS/MS for Simultaneous Determination of Malachite Green and Metabolites Residues in Tilapia" @default.
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• W2967744904 doi "https://doi.org/10.1088/1757-899x/563/5/052062" @default.
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