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• W2968868960 abstract "ABSTRACT Solid state 1 H NMR line‐shape analysis and (double quantum) DQ 1 H NMR experiments have been used to investigate the segmental and polymer chain dynamics as a function of temperature for a series of thermosetting epoxy resins produced using different diamine curing agents. In these thermosets, chemical crosslinks introduce topological constraints leading to residual stresses during curing. Materials containing a unique ferrocene‐based diamine (FcDA) curing agent were evaluated to address the role of the ferrocene fluxional process on the atomic‐level polymer dynamics. At temperatures above the glass transition temperature ( T g ), the DQ 1 H NMR experiments provided a measure of the relative effective crosslink and entanglement densities for these materials and revealed significant polymer chain dynamic heterogeneity in the FcDA‐cured thermosets. © 2019 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2019 , 57 , 1143–1156" @default.
• W2968868960 created "2019-08-22" @default.
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• W2968868960 date "2019-08-09" @default.
• W2968868960 modified "2023-10-17" @default.
• W2968868960 title "Investigating Chain Dynamics in Highly Crosslinked Polymers using Solid‐State ¹H NMR Spectroscopy" @default.
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• W2968868960 doi "https://doi.org/10.1002/polb.24869" @default.
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