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• W2969093153 abstract "Low-coking reactor material technologies are key for improving the performance and sustainability of steam crackers. In an attempt to appraise the coking performance of an alternative Ti-base alloy during ethane steam cracking, an experimental study was performed in a jet stirred reactor under industrially relevant conditions using thermogravimetry (Tgasphase = 1173 K, Ptot = 0.1 MPa, XC2H6 = 70%, and dilution δ = 0.33 kgH2O/kgHC). Initially, a typical pretreatment used for Fe-Ni-Cr alloys was utilized and compared with a pretreatment at increased temperature, aiming at better surface oxidation and thus suppressing coke formation. The results revealed a decrease in coking rates upon high temperature pretreatment of the Ti-base alloy, however, its coking performance was significantly worse compared to the typically used Fe-Ni-Cr alloys, and carbon oxides formation increased by a factor of 30 or more. Moreover, the analyzed coupons showed crack propagation after coking/decoking and cooling down to ambient temperature. Scanning electron microscopy combined with energy-dispersive X-ray spectroscopy indicated that the prompt and unsystematic oxidation of the surface and bulk caused observable crack initiation and propagation due to alloy brittleness. Hence, the tested Ti-base alloy cannot be considered an industrially noteworthy steam cracking reactor alloy." @default.
• W2969093153 created "2019-08-22" @default.
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• W2969093153 date "2019-08-10" @default.
• W2969093153 modified "2023-09-27" @default.
• W2969093153 title "Evaluation of a Ti–Base Alloy as Steam Cracking Reactor Material" @default.
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• W2969093153 doi "https://doi.org/10.3390/ma12162550" @default.
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