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- W2969231738 abstract "Summary A rapid and simple procedure to detect irradiated food containing fat is proposed. This method is based on HS ‐ SPME coupled with GC ‐ MS to determine the presence of a radiolytic product in irradiated meats: 2‐dodecylcyclobutanone (2‐ DCB ) and is proposed as an alternative to EN 1785:2003, which is a long and complex procedure. The qualitative confirmation method is validated on different type of meats: chicken, turkey, duck, beef, pork on both nonirradiated and irradiated samples at different dose levels (0.05, 0.12, 0.5, 1.0 and 3.0 kG y) with a biological X‐ray irradiator. The validation parameters investigated are selectivity, minimum dose level ( MDL ), limit of detection ( LOD ), sensitivity and specificity. The MDL and LOD values were 0.5 kG y and 5.0 ng mL −1 , respectively, for all matrices. No false positives or false negatives occurred, and 100% of samples were correctly identified. The results show that HS ‐ SPME GC ‐ MS is suitable for routine analysis." @default.
- W2969231738 created "2019-08-29" @default.
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- W2969231738 date "2019-09-08" @default.
- W2969231738 modified "2023-10-01" @default.
- W2969231738 title "Validation of an alternative method for the identification of 2‐dodecylcyclebutanone (2‐ <scp>DCB</scp> ) of irradiated meats by solid‐phase microextraction ( <scp>SPME</scp> ) gas chromatography–mass spectrometry ( <scp>GC</scp> ‐ <scp>MS</scp> )" @default.
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- W2969231738 doi "https://doi.org/10.1111/ijfs.14353" @default.
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