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• W2969383977 abstract "The molecular composition of organic matter (OM) and its interaction with minerals play important roles in regulating the fate of carbon and pollutants in soil and in the atmosphere. Clay minerals such as montmorillonite processed with bacteria can imitate the microbial interactions occurring in more complex natural environmental media such as soil and atmospheric particulates. Here, we characterize OMs in multiple phases for bacteria-inoculated montmorillonite clay and atmospheric particulates collected in China. In addition to the traditional 13C cross-polarization magic angle spinning nuclear magnetic resonance (CPMAS NMR) experiments, this study, for the first time, applies both one- and two-dimensional comprehensive multiphase (CMP) NMR to these critical environmental issues. The CMP NMR experimental spectra show that the main OM components in these samples are aliphatics, carbohydrates, and aromatics. These CMP NMR spectra also reveal the biochemical interactions between microbes and clay minerals by identifying the metabolites. CMP NMR can further investigate the states, interfacial/surficial interactions, and dynamics at the molecular/atomic levels since diffusion/relaxation (T2)-edited experiments can distinguish OM with differing sizes and mobilities. Therefore, the mechanism at the atomic/molecular level for environmental biogeochemical interactions can be efficiently probed by CMP NMR experiments. This paper concludes that CMP NMR is a powerful and innovative tool for crucial environmental studies at the molecular/atomic scale, providing not only the composition, phase, and structural identifications but also the interfacial/surficial interaction dynamics involved in environmental geochemical processes." @default.
• W2969383977 created "2019-08-29" @default.
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• W2969383977 date "2019-08-19" @default.
• W2969383977 modified "2023-09-27" @default.
• W2969383977 title "Application of Comprehensive Multiphase NMR To Characterize Organic Matter in Clay and Atmospheric Particulates" @default.
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• W2969383977 doi "https://doi.org/10.1021/acsearthspacechem.9b00148" @default.
• W2969383977 hasPublicationYear "2019" @default.
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