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• W2969916794 abstract "This article describes a home-built scanning electrochemical microscope capable of achieving high areal imaging rates through the use of continuous line probes (CLPs) and compressed sensing (CS) image reconstruction. The CLP is a nonlocal probe consisting of a band electrode, where the achievable spatial resolution is set by the thickness of the band and the achievable imaging rate is largely determined by its width. A combination of linear and rotational motors allows for CLP scanning at different angles over areas up to 25 cm2 to generate the raw signal necessary to reconstruct the desired electrochemical image using CS signal analysis algorithms. Herein, we provide detailed descriptions of CLP fabrication, microscope design, and the procedures used to carry out scanning electrochemical microscopy imaging with CLPs. In order to illustrate the basic operating procedures for the microscope, line scans and images measured in the substrate generation-probe-collection mode for flat samples containing platinum disk electrodes are presented. These exemplary measurements illustrate methods for calibrating the positioning system, positioning and cleaning the CLP, and verifying proper positioning/probe sensitivity along its length." @default.
• W2969916794 created "2019-08-29" @default.
• W2969916794 creator A5006422341 @default.
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• W2969916794 date "2019-08-01" @default.
• W2969916794 modified "2023-09-27" @default.
• W2969916794 title "Design and operation of a scanning electrochemical microscope for imaging with continuous line probes" @default.
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• W2969916794 doi "https://doi.org/10.1063/1.5095951" @default.
• W2969916794 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/31472628" @default.
• W2969916794 hasPublicationYear "2019" @default.
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