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• W2970694256 abstract "1H-Tetrazoles occupy an important role in modern medicinal chemistry, but few methods for their modification exist. Many extant protocols require the use of a difficult to remove N-alkyl-protecting group, precluding the products from use as carboxylate bioisosteres, the major role of tetrazoles in pharmaceuticals. We herein report a convenient, protecting-group-free lithiation-substitution protocol for benzylic tetrazoles. Metalation with n-BuLi at 0 °C followed by electrophilic trapping gave a range of α-functionalized benzyltetrazoles in up to 91% yield." @default.
• W2970694256 created "2019-09-05" @default.
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• W2970694256 date "2019-08-26" @default.
• W2970694256 modified "2023-10-13" @default.
• W2970694256 title "Lithiation Substitution of Unprotected Benzyltetrazoles" @default.
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• W2970694256 doi "https://doi.org/10.1021/acs.orglett.9b02633" @default.
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