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• W2971304529 abstract "Sodium titanate nanotubes (STN) modified by the addition of sodium carbonate (3–10 wt. %) were tested as catalysts for the transesterification of soybean oil with methanol giving good results. Prepared catalysts were characterized by N2 physisorption, X-ray diffraction, FT-IR, temperature-programmed desorption of CO2, scanning and transmission electron microscopy. The STN catalysts modified with sodium carbonate were significantly more active in the transesterification reaction than the reference catalyst containing 5 wt. % of Na2CO3 on alumina. The most active catalyst, STN with 10 wt. % of Na2CO3, resulted in the 97% yield of methyl esters at a short reaction time (30 min) in mild conditions (80 °C). High activity of the prepared catalysts was attributed to a synergetic effect between the support and the deposited sodium carbonate leading to a noticeable increase in the amount of strong basic sites able to generate methoxide anions required for the transformation of triglycerides to methyl esters. According to the FT-IR characterization, the above synergy was attributed to the presence of different types of carbonate species in the alumina and STN-supported catalysts. Upon reutilization, Na2CO3-containing STN catalysts showed a decrease in their activity due to leaching of the active phase in the reaction media." @default.
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• W2971304529 date "2020-08-01" @default.
• W2971304529 modified "2023-10-03" @default.
• W2971304529 title "Synergy between sodium carbonate and sodium titanate nanotubes in the transesterification of soybean oil with methanol" @default.
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• W2971304529 doi "https://doi.org/10.1016/j.cattod.2019.08.027" @default.
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