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• W2971367967 abstract "A synthesis of (+)-xylogiblactone A has been achieved from t-butyl 2-methylbuta-2,3-dienoate in a linear three-step sequence. The key elements of the synthesis include a kinetic resolution of racemic 2-silyoxyaldehyde through the allenoate γ-addition to yield the γ-adduct as a single isomer and the subsequent gold catalysis to form the butenolide core. For a general method, the kinetic resolution of several racemic 2-silyloxyaldehydes is also performed to provide products in high levels of stereoselectivity with unusual anti-Felkin-Anh addition fashion." @default.
• W2971367967 created "2019-09-12" @default.
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• W2971367967 date "2019-09-05" @default.
• W2971367967 modified "2023-10-15" @default.
• W2971367967 title "Kinetic Resolution of Racemic Aldehydes through Asymmetric Allenoate γ-Addition: Synthesis of (+)-Xylogiblactone A" @default.
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• W2971367967 doi "https://doi.org/10.1021/acs.orglett.9b02982" @default.
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