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- W2972698678 abstract "A series of salts of the B12H122− anion has been prepared: a solvent-free (N2H5)2B12H12, its solvates – (N2H5)2B12H12·H2O, (N2H5)2B12H12·2(CH3CN), (N2H5)2B12H12·(CH3OH), and the salt of a protonated azine – [(CH3)2CNNHC(CH3)2]2B12H12. These compounds have been synthesized from the commercially available precursors via one- or two-step procedures and fully identified on the basis of single-crystal and powder X-ray diffraction. At room temperature (N2H5)2B12H12 crystallizes in C2/c space group, with a = 18.480(5) Å, b = 6.5344(19) Å, c = 13.106(4) Å and β = 131.911(16)o, V = 1177.8(7) Å3, Z = 4. While this compound nominally contains ca. 10.7 wt% of hydrogen, it thermally decomposes above 200 °C releasing mainly N2 and NH3, with H2 being only the minor gaseous product. Contrary to the recently reported case of hydrazinates of borohydrides, doping with 5 mol% of FeCl3 does not increase the relative amount of hydrogen significantly, however, it alters the ratio of N2 and NH3." @default.
- W2972698678 created "2019-09-19" @default.
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- W2972698678 date "2019-10-01" @default.
- W2972698678 modified "2023-10-06" @default.
- W2972698678 title "Synthesis, structural characterization and thermal decomposition studies of (N2H5)2B12H12 and its solvates" @default.
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- W2972698678 doi "https://doi.org/10.1016/j.ijhydene.2019.08.158" @default.
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