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• W2972821533 endingPage "14727" @default.
• W2972821533 startingPage "14721" @default.
• W2972821533 abstract "Abstract A more convenient synthesis of the perfluoro alkyl hypofluorite (F 3 C) 3 COF as well as the hitherto unknown (C 2 F 5 )(F 3 C) 2 COF compound is reported. Both hypofluorites can be prepared by use of the corresponding tertiary alcohols R F OH and elemental fluorine in the presence of CsF. An appropriate access to these highly reactive hypofluorites is crucial. The hypofluorites are then transferred into their corresponding perfluoro bisalkyl peroxides R F OOR F [R F =(F 3 C) 3 C, (C 2 F 5 )(F 3 C) 2 C] by treatment with partially fluorinated silver wool. NMR, gas‐phase infrared, and solid‐state Raman spectra of the perfluoro bisalkyl peroxides are presented and their chemical properties are discussed." @default.
• W2972821533 created "2019-09-19" @default.
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• W2972821533 date "2019-10-23" @default.
• W2972821533 modified "2023-10-01" @default.
• W2972821533 title "Perfluoro Alkyl Hypofluorites and Peroxides Revisited" @default.
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• W2972821533 doi "https://doi.org/10.1002/chem.201903620" @default.
• W2972821533 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6899984" @default.
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