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- W2973143075 endingPage "17292" @default.
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- W2973143075 abstract "Replacing toxic isocyanates and petrobased reactants currently employed for polyurethane (PU) synthesis is nowadays a major concern. Among all possible routes to isocyanate-free PUs, aminolysis of cyclic carbonates, leading to polyhydroxyurethanes (PHUs), seems to be one of the most promising pathways. Herein, we discuss the added value brought by the reactive extrusion process on the PHU synthesis. In order to evaluate the benefit and the versatility of the process, three different biscyclic carbonates exhibiting different reactivities (diglycerol dicarbonate, Seb-bCC-ester and one bisCC containing amide function, and Und-6DA-bisCC) were tested in the course of polymerization with different diamines. The PHUs synthesized through reactive extrusion were then compared with the ones obtained through classical bulk polymerizations in terms of kinetics, PHU molar masses, and side reactions, clearly demonstrating the benefit of the extrusion process." @default.
- W2973143075 created "2019-09-19" @default.
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- W2973143075 date "2019-09-10" @default.
- W2973143075 modified "2023-10-17" @default.
- W2973143075 title "Benefit of the Reactive Extrusion in the Course of Polyhydroxyurethanes Synthesis by Aminolysis of Cyclic Carbonates" @default.
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- W2973143075 doi "https://doi.org/10.1021/acssuschemeng.9b04098" @default.
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