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- W2973758001 abstract "A novel polyionic liquid for esterification was synthesized by phenolic condensation. Different characterization techniques were applied, and the result showed that the catalyst had high acidity amount (4.5 mmol/g) and good thermal stability. The decomposition temperature of the polyionic liquid catalyst (PIL-S) was 240 °C, which was fitted to the product of ester. Owing to these good properties, the PIL-S exhibited excellent catalytic activity in esterification. The optimized condition was the 6 wt % catalyst amount, and the ratio of acetic acid to n-butanol was 0.8:1 at 95 °C for 3 h. In the optimized condition, the yield of ester was 97.1%. The PIL-S also has a good catalytic effect in other esterification systems. Compared with commercial resins (Amberlyst 15) and other catalysts, PIL-S showed better catalytic activity. After eight times use, the yield of ester did not decrease obviously (over 94%). The structure of PIL-S remained stable after eight times use." @default.
- W2973758001 created "2019-09-26" @default.
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- W2973758001 date "2019-09-21" @default.
- W2973758001 modified "2023-10-16" @default.
- W2973758001 title "Synthesis of Polyionic Liquid by Phenolic Condensation and Its Application in Esterification" @default.
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- W2973758001 doi "https://doi.org/10.1021/acssuschemeng.9b03859" @default.
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