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- W2974277866 abstract "Abstract 93 Mo is an important long-lived radionuclide in nuclear waste, and is required to be measured during the characterization of decommissioning waste. However, no commercial 93 Mo solution is available to be calibrated and used as standard in the analysis of nuclear waste. This work presents a method for separation of 93 Mo from Nb metal used in cyclotron as a target holder and irradiated with protons for long time. The separation of 93 Mo from Nb matrix was implemented by combination of precipitation and chromatographic separation. The Nb matrix was first removed by precipitating oxides-hydroxides of Nb (e.g. Nb 2 O 5 ) and then by Fe(OH) 3 co-precipitation; Mo in the solution was purified using an alumina (Al 2 O 3 ) column. A decontamination factor of ca. 10 5 was achieved for Nb. A pure carrier-free 93 Mo solution was successfully prepared, and the 93 Mo purity was verified by liquid scintillation spectrometry." @default.
- W2974277866 created "2019-09-26" @default.
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- W2974277866 date "2019-09-16" @default.
- W2974277866 modified "2023-09-23" @default.
- W2974277866 title "Preparation of 93Mo solution using proton irradiated Nb" @default.
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- W2974277866 doi "https://doi.org/10.1007/s10967-019-06758-5" @default.
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