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- W2975722578 abstract "Decalin is a jet fuel additive with high thermal stability and energy density. Herein, we reported a novel method for the preparation of decalin from cyclopentanone, a hemicellulose derived cycloketone. Ethanolamine acetate (EAOAc), an ionic liquid catalyst which can be derived from biomass, was first applied to the self-aldol condensation of cyclopentanone and demonstrated good activity for this reaction. After the optimization of reaction conditions, ∼83.5% carbon yield of 2-cyclopentylidenecyclopentanone was achieved over the EAOAc catalyst. The hydrodeoxygenation of 2-cyclopentylidenecyclopentanone over a physical mixture of Ru/C and H-β zeolite afforded bi(cyclopentane) which could be further isomerized to decalin. Among the screened catalysts, La-Y zeolite exhibited excellent performance for the isomerization process. According to the characterization results, the high activity of La-Y was rationalized by its large medium-strong acid amount and the appropriate ratio of Brønsted acid to Lewis acid. Analogously, branched decalins were synthesized with cyclohexanone using the same procedure." @default.
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- W2975722578 date "2019-09-29" @default.
- W2975722578 modified "2023-09-30" @default.
- W2975722578 title "Synthesis of Decaline-Type Thermal-Stable Jet Fuel Additives with Cycloketones" @default.
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- W2975722578 doi "https://doi.org/10.1021/acssuschemeng.9b04288" @default.
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