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• W2979156744 endingPage "824" @default.
• W2979156744 startingPage "824" @default.
• W2979156744 abstract "Graphene oxide (GO) was used as a catalyst carrier, and after the hydroxyl group in GO was modified by 3-aminopropyltrimethoxysilane (MPTMS), axial coordination and immobilization with homogeneous chiral salenMnCl catalyst were carried out. The immobilized catalysts were characterized in detail by FT–IR, TG–DSC, XPS, EDS, SEM, X-ray, and AAS, and the successful preparation of GO-salenMn was confirmed. Subsequently, the catalytic performance of GO-salenMn for asymmetric epoxidation of α-methyl-styrene, styrene, and indene was examined, and it was observed that GO-salenMn could efficiently catalyze the epoxidation of olefins under an m-CPBA/NMO oxidation system. In addition, α-methyl-styrene was used as a substrate to investigate the recycling performance of GO-salenMn. After repeated use for three times, the catalytic activity and enantioselectivity did not significantly change, and the conversion was still greater than 99%. As the number of cycles increased, the enantioselectivity and chemoselectivity gradually decreased, but even after 10 cycles, the enantiomeric excess was 52%, which was higher than that of the homogeneous counterpart under the same conditions. However, compared to fresh catalysts, the yield decreased from 96.9 to 55.6%." @default.
• W2979156744 created "2019-10-10" @default.
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• W2979156744 date "2019-09-30" @default.
• W2979156744 modified "2023-09-27" @default.
• W2979156744 title "Synthesis of GO-SalenMn and Asymmetric Catalytic Olefin Epoxidation" @default.
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• W2979156744 doi "https://doi.org/10.3390/catal9100824" @default.
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