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• W2980146467 abstract "We report here the development and optimization of a process synthesis for the HIV-1 entry inhibitor BNM-III-170 bis-TFA salt (1). The synthesis features a dynamic-kinetic resolution (DKR) to establish the initial stereogenicity. By taking advantage of significant sequence modifications of our first generation synthesis, inconjunction with the low solubility of late-stage intermediates, the overall efficiency of the synthesis has been significantly improved, now to proceed in an overall yield of 9.64% for the 16-steps, requiring only a single chromatographic separation." @default.
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• W2980146467 date "2019-10-07" @default.
• W2980146467 modified "2023-10-03" @default.
• W2980146467 title "Development of an Effective Scalable Enantioselective Synthesis of the HIV-1 Entry Inhibitor BNM-III-170 as the Bis-trifluoroacetate Salt" @default.
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• W2980146467 doi "https://doi.org/10.1021/acs.oprd.9b00353" @default.
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