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- W2980280981 abstract "Herein, the successful use of a focused ion beam/scanning electron microscope to prepare microsamples of radioactive single crystals for X-ray diffraction analysis is reported. This technique was used to extract and analyze crystalline Pu-containing particles as small as 28 µm 3 from Hanford soil taken from the 216-Z-9 waste crib, which were then crystallographically characterized using single-crystal X-ray diffraction to confirm the cubic structure of PuO 2 . As a systematic proof of concept, the technique was first tested using UO 2 crystals milled into cubic shapes with approximate volumes of 4620, 1331, 125, 8 and 1 µm 3 , in order to empirically determine the crystal size limits for characterization by a laboratory-based diffractometer with a sealed tube Mo or Ag anode X-ray source and a charge-coupled device detector." @default.
- W2980280981 created "2019-10-18" @default.
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- W2980280981 date "2019-10-11" @default.
- W2980280981 modified "2023-10-18" @default.
- W2980280981 title "Extraction of plutonium-containing microcrystals from Hanford soil using a focused ion beam for single-crystal X-ray diffraction analysis" @default.
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- W2980280981 doi "https://doi.org/10.1107/s1600576719012299" @default.
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