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- W2980865525 abstract "N-Heterocyclic carbene (NHC)-catalyzed [3 + 3] annulation of thioamides with modified enals allowing the enantioselective synthesis of functionalized 1,3-thiazin-4-ones is reported. The NHC generated from the chiral triazolium salt was optimal and the reaction is initiated by the thia-Michael addition to catalytically generated α,β-unsaturated acylazolium intermediates derived from 2-bromoenals, followed by intramolecular cyclization. This operationally simple procedure offers a straightforward and rapid access to target compounds in moderate to good yields and enantiomeric ratio values." @default.
- W2980865525 created "2019-10-25" @default.
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- W2980865525 date "2019-10-16" @default.
- W2980865525 modified "2023-10-16" @default.
- W2980865525 title "NHC-Catalyzed [3 + 3] Annulation of Thioamides and Modified Enals for the Enantioselective Synthesis of Functionalized Thiazinones" @default.
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- W2980865525 doi "https://doi.org/10.1021/acs.orglett.9b03188" @default.
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