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• W2981292010 abstract "The analysis of complex mixtures is an important but often intractable problem. When species contain sparse fluorine atoms, NMR spectra of fluorine-containing spin systems can be efficiently extracted from an intact mixture using the recently proposed FESTA (Fluorine-Edited Selective TOCSY Acquisition) methodology. Here an alternative approach to the existing selective reverse INEPT FESTA (SRI-FESTA) experiment is described, based on the use of a modulated spin echo for the initial excitation. MODO-FESTA (modulated echo FESTA) is simpler and has a significant sensitivity advantage over SRI-FESTA. Comparisons are presented of the relative sensitivity and spectral purity of the two types of methods." @default.
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• W2981292010 date "2019-12-17" @default.
• W2981292010 modified "2023-10-16" @default.
• W2981292010 title "Improving the Sensitivity of FESTA Methods for the Analysis of Fluorinated Mixtures" @default.
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• W2981292010 doi "https://doi.org/10.1021/acs.analchem.9b04924" @default.
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