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• W2981856565 abstract "A green route is presented to synthesize bio-based nonisocyanate thermoplastic polyoxamide-ureas (POXAUs) containing flexible poly(propylene oxide) segments. A hexanedioxamide-diester (HDODE) was synthesized from the reaction of 1,6-hexanediamine with excessive diethyl oxalate. Four H2N– terminated polyoxamide prepolymers (PrePOXAs) were synthesized through melt polycondensation of HDODE with O,O′-bis(2-aminopropyl) poly(propylene glycol). Chain extension of PrePOXAs was conducted with bis(hydroxyethyl) hexanediurethane as a chain extender, and four chain-extended POXAs or POXAUs were prepared. The POXAUs were characterized by size exclusion chromatography, Fourier transform infrared, 1H NMR, wide-angle X-ray scattering, differential scanning calorimetry, thermogravimetric analysis, and tensile testing. POXAUs show Mn up to 29 900 g mol–1, melting temperature from 148 to 156 °C, initial decomposition over 242 °C, tensile strength up to 60 MPa, and elongation at break from 8 to 16%. Crystallized bio-based thermoplastic poly(oxamide urea)s with excellent thermal and mechanical properties were successfully synthesized through a nonisocyanate route." @default.
• W2981856565 created "2019-11-01" @default.
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• W2981856565 date "2019-10-24" @default.
• W2981856565 modified "2023-10-14" @default.
• W2981856565 title "Synthesis and Properties of Bio-Based Nonisocyanate Thermoplastic Polyoxamide-Ureas" @default.
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• W2981856565 doi "https://doi.org/10.1021/acs.iecr.9b04617" @default.
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