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- W2986409312 abstract "The structure of (CH3(OCH2CH2)2OCH3)2LiSbF6 was solved by single-crystal X-ray diffraction techniques. The compound crystallizes in the orthorhombic Pccn space group with a unit cell containing four lithium ions, each of which is coordinated by two CH3(OCH2CH2)2OCH3 or diglyme molecules. The SbF6- anion does not directly interact with the cation, similar to its isolated environment in crystalline, high molecular weight P(EO)6LiSbF6. A comparative vibrational spectroscopic study of (CH3(OCH2CH2)2OCH3)2LiSbF6 and P(EO)6LiSbF6 demonstrated that the ethylene oxide vibrations in both systems were essentially decoupled and could be analyzed in terms of a single diglyme or PEO molecule, respectively. A spectroscopic comparison of the isostructural crystalline P(EO)6LiAsF6, P(EO)6LiPF6, and P(EO)6LiSb6 compounds demonstrated that the band frequencies in the former compound are consistently higher by a few wavenumbers than those of the latter two systems. This was attributed to the effect of the Li−O distances." @default.
- W2986409312 created "2019-11-22" @default.
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- W2986409312 date "2003-09-20" @default.
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- W2986409312 title "Vibrational Study of the Crystalline Phases of (CH<sub>3</sub>(OCH<sub>2</sub>CH<sub>2</sub>)<sub>2</sub>OCH<sub>3</sub>)<sub>2</sub>LiSbF<sub>6</sub> and P(EO)<sub>6</sub>LiMF<sub>6</sub> (M = P, As, Sb)" @default.
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- W2986409312 doi "https://doi.org/10.1021/jp030199c" @default.
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