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- W2989359610 abstract "Amino acid derivatives undergo non-Kolbe electrolysis to afford enantiomerically enriched α-alkoxyamino derivatives through intermediate chiral carbenium ions. The products contain N,O-acetals which are important structural motifs found in bioactive natural products. The reaction is performed in a continuous flow electrochemical reactor coupled to a 2D-HPLC for immediate online analysis. This allowed a fast screening of temperature, electrode material, current, flow-rate and concentration in a DoE approach. The combination with online HPLC demonstrates that also stereoselective reactions can benefit from a hugely accelerated optimisation by combining flow electrochemistry with multidimensional analysis." @default.
- W2989359610 created "2019-11-22" @default.
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- W2989359610 date "2019-11-21" @default.
- W2989359610 modified "2023-09-23" @default.
- W2989359610 title "Memory of Chirality in Flow Electrochemistry: Fast Optimisation with DoE and Online 2D‐HPLC" @default.
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- W2989359610 doi "https://doi.org/10.1002/chem.201904711" @default.
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