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- W2989615317 abstract "After crystallization during ionothermal syntheses in phosphonium-containing ionic liquids, the structure of (NH 4 ) 3 Al 2 (PO 4 ) 3 [triammonium dialuminum tris(phosphate)] was refined on the basis of powder X-ray diffraction data from a synchrotron source. (NH 4 ) 3 Al 2 (PO 4 ) 3 is a member of the structural family with formula A 3 Al 2 (PO 4 ) 3 , where A is a group 1 element, and of which the NH 4 , K, and Rb forms were previously known. The NH 4 form is isostructural with the K form, and was previously solved from single-crystal X-ray data when the material (SIZ-2) crystallized from a choline-containing eutectic mixture [Cooper et al. (2004). Nature , 430 , 1012–1017]. Our independent refinement incorporates NH 4 groups and shows that these NH 4 groups are hydrogen bonded to framework O atoms present in rings containing 12 T sites in a channel along the c- axis direction. We describe structural details of (NH 4 ) 3 Al 2 (PO 4 ) 3 and discuss differences with respect to isostructural forms." @default.
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- W2989615317 date "2019-11-19" @default.
- W2989615317 modified "2023-09-26" @default.
- W2989615317 title "Structure refinement of (NH4)3Al2(PO4)3 prepared by ionothermal synthesis in phosphonium based ionic liquids – a redetermination" @default.
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- W2989615317 doi "https://doi.org/10.1107/s2056989019015330" @default.
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