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- W2990682074 abstract "Abstract A series of nickel‐decorated covalent organic frameworks, NiCl@RIO‐12, were prepared using the post‐synthetic modification strategy, that is, by reacting NiCl 2 with pristine RIO‐12 under alkaline conditions. Interestingly, they retained their crystallinity and the amount of nickel incorporated could be tuned from 3.6 to 25 wt % according to the reaction conditions. The incorporation of a higher amount of nickel in NiCl@RIO‐12 consistently led to a lower Brunauer–Emmett–Teller surface area. Additionally, no agglomeration of nickel particles was found and a relatively homogeneous dispersion of nickel could be ascertained by SEM and TEM‐EDS. The paramagnetic material exhibited promising catalytic activity in Suzuki–Miyaura cross‐coupling under microwave heating. Thus, NiCl@RIO‐12 notably demonstrated good thermal stability and its recyclability showed no substantial loss of activity after 3 cycles." @default.
- W2990682074 created "2019-12-05" @default.
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- W2990682074 date "2020-01-30" @default.
- W2990682074 modified "2023-10-17" @default.
- W2990682074 title "Design, Synthesis and Characterization of Nickel‐Functionalized Covalent Organic Framework NiCl@RIO‐12 for Heterogeneous Suzuki–Miyaura Catalysis" @default.
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- W2990682074 doi "https://doi.org/10.1002/chem.201904845" @default.
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