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• W2991489234 endingPage "012140" @default.
• W2991489234 startingPage "012140" @default.
• W2991489234 abstract "Abstract The paper presents the results of the research of structure of a thin film CuO/Ce 0.9 Gd 0.1 O 2-δ (CuO/GDC) anode for solid oxide fuel cells (SOFCs) prepared by magnetron sputtering. Cu-based anode materials of SOFCs are of great interest because they exhibit greater tolerance to sulfur-containing fuels than the widely used Ni-based composite anodes. After deposition, annealing in air and reducing atmospheres, the composition, microstructure and crystallinity of the films were characterized using energy dispersive X-Ray spectroscopy, scanning electron microscopy and X-ray diffractometry, respectively. The as-deposited film consists of cubic fluorite structures of GDC and Cu 2 O and has a dense, homogeneous structure, in which Cu is evenly distributed over the volume of the film. However, it was shown that, strong Cu segregation is observed in CuO/GDC films, after reduction in hydrogen at a temperature of 750 °C, with the formation of massive agglomerates on the surface. The influence of pre-calcination of the as-deposited films at 1000 °C and 1200 °C on their structure was studied. It is shown that annealing at a temperature of 1000 °C does not prevent the agglomeration of Cu in a reducing atmosphere, while Cu evaporation is observed if annealing temperature is 1200 °C." @default.
• W2991489234 created "2019-12-05" @default.
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• W2991489234 date "2019-11-01" @default.
• W2991489234 modified "2023-10-18" @default.
• W2991489234 title "Structural features of the magnetron sputtered CuO/GDC anodes for solid oxide fuel cells" @default.
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• W2991489234 doi "https://doi.org/10.1088/1742-6596/1393/1/012140" @default.
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