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• W2994348803 endingPage "119310" @default.
• W2994348803 startingPage "119310" @default.
• W2994348803 abstract "Three new metal–organic complexes [Cd(TIPA)(suc)0.5(NO3)·½H2O]n (1), [Ni(TIPA)(tda)0.5(H2O)·¼H2O]n (2) and [Cd(TIPA)(tda)0.5·1½H2O] (3) were synthesized via rigid tripodal ligand tris(4-(1H-imidazol-1-yl)phenyl)amine (TIPA) and three dicarboxylic acids either succinic acid (H2suc) or 2,5-thiophenedicarboxylic acid (H2tda). Crystallographic data for 1–3 reveal three-dimensional (3D) networks and channels in the structures. The structure of 2 is unique featuring an interpenetrating 2D network, 2D + 2D → 3D, with the two associated 2D networks existing in two opposite spiral channels. TGA plots exhibit a loss of mass corresponding to the loss of the solvated water molecules in the 100–200 °C temperature region and begin to lose additional fragments only at T > 300 °C revealing the robust nature of the 3D framework in the complexes. The metal-organic frameworks (MOFs) are screened for their potential application in the detection and removal of environmentally hazardous industrial pollutants. Fluorescence emission spectra for 1 and 2 show that the two MOFs are capable of sensing nitrobenzene (NB), with the nickel complex 2 exhibiting significantly higher sensing ability. Powder XRD data measured for 1 and 2 and those of NB-treated 1 and 2 show significant differences in their patterns, providing further support for the strong interaction between the MOF complexes and NB. The fluorescence emission observed for 1 is more effectively quenched by the presence of Fe3+ than any of 17 other metal ions investigated. Complex 3 possesses some ability to adsorb inorganic pollutants." @default.
• W2994348803 created "2019-12-13" @default.
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• W2994348803 date "2020-03-01" @default.
• W2994348803 modified "2023-10-04" @default.
• W2994348803 title "Three new metal complexes with imidazole-containing tripodal ligands as fluorophores for nitroaromatics- and ion-selective sensing" @default.
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• W2994348803 doi "https://doi.org/10.1016/j.ica.2019.119310" @default.
• W2994348803 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/7453589" @default.
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