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• W2994832313 endingPage "107724" @default.
• W2994832313 startingPage "107724" @default.
• W2994832313 abstract "Systematic vanadosilicate syntheses were performed using derivatives of 2,6-dimethylpiperidine as organic structure-directing agents (SDAs). Physicochemical analyses of the vanadosilicate materials obtained were carried out by X-ray diffraction (XRD), Raman spectroscopy, infrared (IR) spectroscopy, UV–visible (UV–Vis) spectroscopy, and solid-state NMR spectroscopy (29Si and 51V MAS NMR). The experimental results indicated that the presence of the organic templates had different effects on the final phases of the synthesized vanadosilicates. The XRD results showed that 1,1,2,6-tetramethylpiperidinium (SDA 1) favored synthesis of the known AM-6 vanadosilicates, isostructural to the ETS-10 titanosilicate, while the other organic templates 1,1-diethyl-2,6-dimethylpiperidinium (SDA 2), 6,10-dimethyl-5-azoniaspiro[4.5]decane (SDA 3), and 1,5-dimethyl-6-azoniaspiro[5.5]undecane (SDA 4) directed the formation of vanadosilicates with different phases, such as EVS-10. Strong Raman bands at 870 and 1035 cm−1 indicated vibrational modes associated with the highly symmetric vanadia octahedra. Chemical shifts at −96 ppm (29Si MAS NMR), −610, and −570 ppm (51V MAS NMR) provided further evidence of the incorporation of vanadium into the structures of the vanadosilicates prepared using these novel derivatives of 2,6-dimethylpiperidinium cations as SDAs." @default.
• W2994832313 created "2019-12-26" @default.
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• W2994832313 date "2020-02-01" @default.
• W2994832313 modified "2023-10-12" @default.
• W2994832313 title "Synthesis of ETS-10-like vanadosilicates using 2,6-dimethylpiperidinium cation derivatives as organic templates" @default.
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• W2994832313 doi "https://doi.org/10.1016/j.inoche.2019.107724" @default.
• W2994832313 hasPublicationYear "2020" @default.
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