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- W2996137024 abstract "Bio-based poly(isosorbide 2,5-furandicarboxylate-co-ε-caprolactone) (PIFCL) copolyesters were synthesized from 2,5-furandicarboxylic acid, isosorbide and ε-caprolactone. The obtained copolyesters were characterized by 1H NMR, 13C NMR, intrinsic viscosity, GPC, DSC, TGA and tensile testing. The NMR characterization results confirmed the insertion of lactones units into poly(isosorbide 2,5-furandicarboxylate) (PIF) chains. All PIFCL copolyesters were amorphous with TD, 5% higher than 300 °C. The glass transition temperatures of PIFCLs with FDCA molar ratio from 74% to 45% were within the range of 132.1 °C and 72.4 °C. Tensile testing revealed that introduction of ε-caprolactone into PIF chain imparted PIFCL with excellent mechanical performance, typically, PIFCL polyseter with FDCA molar ratio of 45% had a Young's modulus 858 ± 92 MPa, a tensile strength 44 ± 4 MPa and an elongation at break 480 ± 45%." @default.
- W2996137024 created "2019-12-26" @default.
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- W2996137024 date "2020-01-01" @default.
- W2996137024 modified "2023-09-24" @default.
- W2996137024 title "Synthesis and properties of poly(isosorbide 2,5-furandicarboxylate-co-ε-caprolactone) copolyesters" @default.
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- W2996137024 doi "https://doi.org/10.1016/j.polymertesting.2019.106284" @default.
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